I-N-Benzyl-N-ethylaniline

1 Luwuketshezi oluphuzi olukhanyayo olunamafutha, oluncibilikayo ku-ethanol nakwezinye izinyibilikisi eziphilayo, olungancibiliki emanzini.

2, Indlela yokukhiqiza itholakala ngokuphendula i-ethyl aniline kanye ne-benzyl chloride. Eketheni elinomugqa we-lead, engeza i-ethyl aniline, engeza i-benzyl chloride ngenkathi uphola, uvuselele amahora ayi-10, bese ugcina ufudumele ku-100°C amahora ayi-12. Ngemva kokugezwa ngesisombululo se-sodium hydroxide, umkhiqizo oqediwe utholakala ngokuhluzwa nge-vacuum. I-Diethylaniline ingasetshenziswa futhi njengezinto zokusetshenziswa. Isilinganiso se-molar se-diethylaniline ku-benzyl chloride singu-2:1. Engeza u-1% wenani lokuphakelwa kwe-diethylaniline ukuze uyixube ne-iodine, uphendule ku-150℃ amahora angama-20, bese uxuba nge-vacuum ukuze uthole umkhiqizo oqediwe.

3, Isetshenziswa njengodayi ophakathi nendawo. Isetshenziselwa ukwenza i-SF eluhlaza okwesibhakabhaka okune-acidic kanye nezinye izidayi eziluhlaza okwesibhakabhaka.

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